Utilization of microflow reactors to carry out synthetically useful organic photochemical reactions |
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| Institution: | 1. Graduate School of Materials Science, Nara Institute of Science and Technology (NAIST), 8916-5 Takayamacho, Ikoma, Nara 630-0101, Japan;2. Department of Applied Chemistry, Graduate School of Engineering, Osaka Prefecture University, 1-1 Gakuen-cho, Nakaku, Sakai, Osaka 599-8531, Japan;3. The Research Institute for Molecular Electronic Devices (RIMED), Osaka Prefecture University, 1-1 Gakuen-cho, Nakaku, Sakai, Osaka 599-8531, Japan;1. School of Chemistry and Chemical Engineering, Tianjin University of Technology, Tianjin 300384, PR China;2. Graduate School of Materials Science, Nara Institute of Science and Technology (NAIST), 8916-5 Takayama, Ikoma, Nara 630-0192, Japan;1. International Academy of Optoelectronics at Zhaoqing, South China Normal University, Zhaoqing, 526238 Guangdong, PR China;2. Guangdong Provincial Key Laboratory of Optical Information Materials and Technology & Institute of Electronic Paper Displays, South China Academy of Advanced Optoelectronics, South China Normal University, Guangzhou 510006, PR China;3. ARC Centre of Excellence in Exciton Science, School of Chemistry, University of Melbourne, Parkville, VIC 3010, Australia;4. Institute of Fundamental Technological Research, Polish Academy of Sciences, 02-106 Warsaw, Poland;5. School of Information and Optoelectronic Science and Engineering, South China Normal University, Guangzhou, 510006 Guangdong, PR China;1. Physical and Materials Chemistry Division, CSIR-National Chemical Laboratory, Pune, 411 008, India;2. Chemical Engineering & Process Development Division, CSIR-National Chemical Laboratory, Pune, 411 008, India;3. Academy of Scientific and Innovative Research, New Delhi, 110025, India;1. Nanomaterials, Catalysis & Electrochemistry (NCE), Department of Chemical Engineering, University of Liège, B-4000 Liège, Belgium;2. Center for Integrated Technology and Organic Synthesis (CiTOS), Department of Chemistry, University of Liège, B-4000 Liège, Belgium;3. GRASP-Biophotonics, Department of Physics, University of Liège, B-4000 Liège, Belgium;1. Chemical Engineering Department, National Research Centre, Egypt;2. Chemical Science and Engineering Department, Tokyo Institute of Technology, Japan;3. Energy Resources Engineering Department, Egypt-Japan University of Science and Technology, Egypt |
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| Abstract: | This review focuses on recent advances that have been made in conducting synthetically useful organic photochemical reactions by using microflow reactors. Attention is given to the utilization of this technique in the “scale-up” of a variety of photochemical processes including intermolecular photocycloadditions, intramolecular photocycloadditions and photocyclizations, photoadditions, photoreductions, photoisomerizations, photosubstitutions, photooxidations, photorearrangements, and heterogeneous photocatalytic reactions. In many examples, the use of the microflow method is compared to those carried out in batch systems. Finally, advantages and disadvantages of microflow photoreactions along with the possible employment of this approach to scale-up industrial photochemical processes are discussed. |
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| Keywords: | Microreactor Flow chemistry Microreactor photochemistry Synthetic organic photochemistry Slug flow |
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