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Double-acquisition: utilization of discarded coherences in a 2D separation experiment using the States method
Authors:Fukuchi Masashi  Inukai Munehiro  Takeda Kazuyuki  Takegoshi K
Affiliation:aDivision of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwake-cho, Sakyo-ku, Kyoto 606-8502, Japan;bDivision of Advanced Electronics and Optical Science, Graduate School of Engineering Science, Osaka University, Toyonaka, Osaka 560-8531, Japan
Abstract:We propose a new data-acquisition scheme for 2D separation experiments to save the spectrometer time by 1/2. This scheme, referred to as a double-acquisition scheme, is applicable to most of separation experiments with the hypercomplex time-domain data-acquisition scheme (the States method) for data collection.
Keywords:Double-acquisition   2D separation experiment   Dipolar recoupling   Chemical-shift anisotropy recoupling
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