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Determination of peptide φ angles in solids by relayed anisotropy correlation NMR |
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| Authors: | Yoshitaka Ishii Koichi Hirao Takehiko Terao Tsutomu Terauchi Makoto Oba Kozaburo Nishiyama Masatsune Kainosho |
| Institution: | a Department of Chemistry, Graduate School of Science, Kyoto University, Kyoto 606-8502, Japan b Department of Material Science and Technology, Tokai University, 317 Nishino, Numazu, Shizuoka 410-03, Japan c Department of Bioscience, School of Science and Engineering, Teikyo University, Toyosatodai 1-1, Utsunomiya 320, Japan d Toray Research Center, Shiga, 3-7 Sonoyama 3-chome, Otsu, Shiga 520, Japan |
| Abstract: | A solid state NMR method is presented for determination of a backbone dihedral angle φ in peptides, being based on the previously reported method, relayed anisotropy correlation (RACO) NMR Y. Ishii et al., Chem. Phys. Lett. 256 (1996) 133]. In the present method, the |
| Keywords: | 2D MAS NMR 2D powder pattern Dihedral angle |
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