Synthesis of 3-substituted 4-imino-4,5-dihydro-1,2,3-triazole 1-oxides and 4-amino-1,2,3-triazole 1-oxides. Crystal and molecular structure of 4-imino-5,5-dimethyl-3-phenyl-4,5-dihydro-1,2,3-triazole 1-oxide |
| |
| Authors: | S. G. Zlotin O. V. Prokshits M. O. Dekaprilevich D. S. Yufit O. A. Lukyanov Yu. T. Struchkov |
| |
| Affiliation: | (1) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 117913 Moscow, Russian Federation;(2) A. N. Nesmeyanov Institute of Organoelemenl Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 117813 Moscow, Russian Federation |
| |
| Abstract: | A new procedure for the synthesis of triazole N-oxides, based on base-induced intramolecular cyclization of 1-( -cyanoalkyl)-3-aryl(hetaryl)triazen-1-oxides, is proposed. An X-ray study of 4-imino-5,5-dimethyl-3-phenyl-4,5-dihydro-1,2,3-triazole 1-oxide was carried out.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 4, pp. 746–751, April, 1993. |
| |
| Keywords: | 1,2,3-triazole N-oxides, synthesis triazene i-oxides, bases 4-imino-5,5-dimethyl-3-phenyl-4,5-dihydro-1,2,3-triazole 1-oxide, X-ray study |
| 本文献已被 SpringerLink 等数据库收录！ |
|
