Calculations and interpretation of the results of stoichiographic analysis of solid multi-element multi-phase compounds and materials |
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Authors: | V V Malakhov A A Vlasov |
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Institution: | 1.Boreskov Institute of Catalysis, Siberian Division,Russian Academy of Sciences,Novosibirsk,Russia |
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Abstract: | Methods and approaches to the calculations and interpretation of the results of stoichiographic analysis of solid multi-element
multi-phase compounds and materials using the flow mode of the differential dissolution (DD) method are reported. Special features of calculationls as well as the objective reasons for the necessity of obtaining more
or less precise results of stoichiographic calculations are discussed. The details of the procedure of stoichiographic calculations,
refinement, and interpretation of the results are considered on an example of the DD-analysis of the Co-Ni-Fe-Bi-K-P-Mo-O/SiO2-catalyst for the selective oxidation and oxidative ammonolysis of hydrocarbons. The specific details and methods used for
the estimation of the performance characteristics of the DD analytical procedure are discussed. |
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