| 超高交联吸附树脂柱色谱法分离提纯喜树碱及喜果甙 |
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| 引用本文： | 王瑞芳,史作清,施荣富,欧来良,王重,刘二伟.超高交联吸附树脂柱色谱法分离提纯喜树碱及喜果甙[J].离子交换与吸附,2002,18(5):412-418. |
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| 作者姓名： | 王瑞芳 史作清 施荣富 欧来良 王重 刘二伟 |
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| 作者单位： | 吸附分离功能高分子材料国家重点实验室,高分子化学研究所,天津,300071 |
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| 基金项目： | 国家自然科学基金 (No: 29974015) |
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| 摘 要： | 本文比较了所合成的8种大孔超高交联吸附树脂对喜树果提取液中喜树碱和喜果甙的吸附性能及柱层析分离效果。结果表明，经超高效联树脂的层析分离，喜树碱的质量分数可提高到约15％，喜果甙的质量分数可提高到约60％。
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| 关 键 词： | 交联吸附树脂 柱色谱法 分离 提纯 喜树碱 喜果甙 吸附性能 层析分离 植物药 有效成分 |
| 文章编号： | 1001-5493(2002)05-0412-07 |
| 修稿时间： | 2002年8月1日 |
CHROMATOGRAPHIC SEPARATION OF CAMPTOTHECINE AND VINCOSIDE-LACTAM WITH MACROPOROUS HYPERCROSSLINKED RESINS |
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| WANG Ruifang SHI Zuoqing SHI Rongfu Ou Lailiang Wang Zhong Liu Erwei State Key Laboratory of Functional Polymeric Materials for Adorption Separation Institute of Polymer Chemistry,NanKai University,TianJin ,China.CHROMATOGRAPHIC SEPARATION OF CAMPTOTHECINE AND VINCOSIDE-LACTAM WITH MACROPOROUS HYPERCROSSLINKED RESINS[J].Ion Exchange and Adsorption,2002,18(5):412-418. |
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| Authors: | WANG Ruifang SHI Zuoqing SHI Rongfu Ou Lailiang Wang Zhong Liu Erwei State Key Laboratory of Functional Polymeric Materials for Adorption Separation Institute of Polymer Chemistry NanKai University TianJin China |
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| Institution: | WANG Ruifang SHI Zuoqing SHI Rongfu Ou Lailiang Wang Zhong Liu Erwei State Key Laboratory of Functional Polymeric Materials for Adorption Separation Institute of Polymer Chemistry,NanKai University,TianJin 300071,China |
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| Abstract: | The performance of adsorption and chromatographic separation for camptothecine and vincoside-lactam with eight macroporous hypercrosslinked resins self-maded was compared in this paper. The results showed the content of camptothecin and vincoside-lactam could be improved to about 15% and 60% respectively after chromatographic separation with these kind resins. |
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| Keywords: | Camptothecine Vincoside-lactam Macroporous hyper-crosslinked resin Adsorption performance Chromatographic separation |
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