| 苯氧乙酸烯丙酯的合成 |
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| 引用本文： | 孟庆朝,董玉环.苯氧乙酸烯丙酯的合成[J].合成化学,2004,12(2):201-203. |
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| 作者姓名： | 孟庆朝 董玉环 |
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| 作者单位： | 唐山师范学院化学系,河北,唐山,063000;唐山师范学院化学系,河北,唐山,063000 |
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| 摘 要： | 对苯酚和氯乙酸的Williamson反应加以改进，使苯氧乙酸的收率达到95．4％。并以苯氧乙酸和烯丙醇为原料，活性碳负载磷钨酸为催化剂，合成了苯氧乙酸烯丙酯。考察了两个反应的主要影响因素。
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| 关 键 词： | 苯氧乙酸 苯氧乙酸烯丙酯 活性碳负载磷钨酸 催化 |
| 文章编号： | 1005-1511(2004)02-0201-03 |
| 修稿时间： | 2003年3月24日 |
Synthesis of Allyl Phenoxyacetate |
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| MENG Qing-zhao,DONG Yu-huan.Synthesis of Allyl Phenoxyacetate[J].Chinese Journal of Synthetic Chemistry,2004,12(2):201-203. |
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| Authors: | MENG Qing-zhao DONG Yu-huan |
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| Abstract: | An improved synthesis of phenoxyacetic acid by Williamson reaction of phenol and chloroacetic acid with the yield of 95.4% was reported. And allyl phenoxyacetate was synthesized by esterification of phenoxyacetic acid and allyl alcohol catalyzed by phosphotungstic acid supported on activated carbon. The major effect factors on the two reactions were also studied. |
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| Keywords: | phenoxyacetic acid allyl phenoxyacetate phosphotungstic acid supported on activated carbon catalysis |
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