Mössbauer and X-ray diffraction studies of mechanically alloyed Fe-Al |
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Authors: | Elżbieta Jartych Jan Krzysztof Zurawicz Dariusz Oleszak Jan Sarzyński Mieczysław Bundzyński |
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Affiliation: | (1) Department of Physics, Technical University of Lublin, ulica Nadbystrzycka 38, 20-618 Lublin, Poland;(2) Department of Materials Science and Engineering, Warsaw University of Technology, ulica Narbutta 85, 02-524 Warsaw, Poland;(3) Institute of Physics, University of Maria Curie-Sklodowska, Plac. M. Curie-Sklodowskiej 1, 20-031 Lublin, Poland |
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Abstract: | Powder samples of Fe25Al75 were prepared by the mechanical alloying method. Mössbauer effect, X-ray diffraction and DSC measurements indicate that Fe and Al crystalline powder transform into Fe-Al amorphous powder with increasing milling time. The X-ray diffraction patterns of the milled Fe25Al75 do not clearly show a sign of the existence of the intermetallic phases or Fe-Al solid solution. However, Mössbauer measurements reveal two sites with hyperfine magnetic fields 30.2 and 26.0 T. These sites form locally during the milling process and then they disappear. |
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