| UPLC-MS-MS法快速测定玉米中的黄曲霉毒素B1 |
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| 引用本文： | 于成广,黄辉.UPLC-MS-MS法快速测定玉米中的黄曲霉毒素B1[J].化学分析计量,2012,21(2):81-83. |
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| 作者姓名： | 于成广 黄辉 |
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| 作者单位： | 1. 济南市农业质量检测中心,济南,250002
2. 中国兵器工业集团第五三研究所,济南,250031 |
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| 摘 要： | 采用高效液相色谱-串联质谱法检测玉米中的黄曲霉毒素B1。对样品前处理条件、净化和分离条件进行了优化，黄曲霉毒素B1检出限为0．02μg／kg，回收率为83．8％～95．7％。建立的方法简便、快速、灵敏度高，能够满足玉米中痕量黄曲霉毒素B1农残的高灵敏测定要求。
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| 关 键 词： | 黄曲霉毒素B1 高效液相色谱串联质谱 玉米 |
Ultra-High Performance Liquid Chromatography Tandem Mass Spectrometry for Rapid Determination of Aflatoxin B1 in Corn |
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| Yu Chengguang
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Huang Hui.Ultra-High Performance Liquid Chromatography Tandem Mass Spectrometry for Rapid Determination of Aflatoxin B1 in Corn[J].Chemical Analysis And Meterage,2012,21(2):81-83. |
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| Authors: | Yu Chengguang Huang Hui |
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| Institution: | Yu Chengguang Huang Hui(Test Centre for Agriculture quality of Jinan,Jinan 250002,China)(CNGC Institue 53,Jinan 250031,China) |
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| Abstract: | An analytical method for the determination of aflatoxin B1 in corn by ultra-high performance liquid chromatography tandem mass spectrometry was developed.Sample pretreatment methods and depuration conditions were optimized.The detection limit of aflatoxin B1 was 0.02 μg/kg.The recoveries were 83.8% – 95.7%.The results indicated that the method developed is simple,rapid,sensitive,which is suit for the analysis of aflatoxin B1 pesticides in corn. |
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| Keywords: | aflatoxin B1 HPLC-MS/MS corn |
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