合成氟金云母单晶缺陷的X射线研究

本文报道了人工合成大面积氟金云母单晶中缺陷的X射线研究结果。X射线劳厄法的研究表明,在合成云母中存在着较大程度的一维无序,并因而出现许多堆垛错排区及其亚晶界。X射线衍射形貌术的研究表明,合成云母中的亚晶界和位错线大部分是从晶种起源并向生长表面的法线方向延伸的。晶体的靠近表面的区域缺陷较密集,中心部分较少。探讨了合成云母与天然云母中缺陷分布的差别。对用于制作电容器的合成云母片的缺陷与性能的关系作了分析和讨论。 关键词：

A X-RAY STUDY OF IMPERFECTION IN SYNTHETIC FLUOROPHLOGOPITE CRYSTAL

This paper describes the results of X-ray study of imperfection in the single crystal of large area synthetic fluorophlogopite. By using X-ray Laue method, it is showed that in synthetic mica there is a greater degree of one-dimensional disorder, and therefore there are a number of disarranged regions of stacking sequence and their boundaries. The X-ray diffraction topography method shows that most of sub-grain boundaries and dislocations originate from the seed and run normal to the growth surfaces. The density of crystal defects in the region near the crystal surface is greater than that in the center. The difference in the distribution of defects between synthetic mica and natural mica was investigated. The relationships between defects in synthetic mica plate and their performances as used to construct condenser were also studied and discussed.