Results of thermal analysis for investigation of salt hydrates as latent heat-storage materials |
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Authors: | R Naumann H -H Emons |
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Institution: | (1) Bergakademie Freiberg, Sektion Chemie Freiberg, 9200, DDR |
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Abstract: | DTA and DSC methods and quasi-isothermal and quasi-isobaric thermogravimetry are of great importance in the investigation of salt hydrates as latent heat-storage materials. However, the transferability of the DTA and DSC results is given only for application in static latent heatstorage units. Special calorimetric methods adapted to the storage principle are preferred for the study of salt hydrates under dynamic storage conditions. The findings are discussed in connection with the examples of Na2SO4·10H2O, CH3COONa·3H2O, Na2S·9H2O, Na2S·5H2O, Mg(NO3)2·6H2O, MgCl2·6H2O and the eutectic mixture of Mg(NO3)2·6H2O-MgCl2·6H2O.
Zusammenfassung Bei der Untersuchung von Salzhydraten als Latentwärmespeichermaterialien besitzen DTA-, DSC-Methoden und die quasi-isotherme und quasi-isobare Thermogravimetrie eine wesentliche Bedeutung. Die Übertragbarkeit der DTA- und DSC-Ergebnisse ist jedoch nur für den Einsatz in statischen latentwärmespeichern gegeben. Für das Studium der Salzhydrate under dynamischen Speicherbedingungen werden spezielle, dem Speicherprinzip angepaßte kalorimetrische Methoden bevorzugt. Die Aussagen werden an den Beispielen Na2SO4·10H2O, CH3COONa·3H2O, Na2S·9H2O, Na2S·5H2O, Mg(NO3)2·6H2O, MgCl2·6H2O und der eutektischen Mischung von Mg(NO3)2·6H2O-MgCl2·6H2O diskutiert.
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![dcy](/content/x7764372l6861431/xxlarge1076.gif) ![acy](/content/x7764372l6861431/xxlarge1072.gif) ![ncy](/content/x7764372l6861431/xxlarge1085.gif) ![ycy](/content/x7764372l6861431/xxlarge1099.gif) ![ocy](/content/x7764372l6861431/xxlarge1086.gif) ![bcy](/content/x7764372l6861431/xxlarge1073.gif) ![scy](/content/x7764372l6861431/xxlarge1089.gif) ![ucy](/content/x7764372l6861431/xxlarge1091.gif) ![zhcy](/content/x7764372l6861431/xxlarge1078.gif) ![dcy](/content/x7764372l6861431/xxlarge1076.gif) ![iecy](/content/x7764372l6861431/xxlarge1077.gif) ![ncy](/content/x7764372l6861431/xxlarge1085.gif) ![ncy](/content/x7764372l6861431/xxlarge1085.gif) ![pcy](/content/x7764372l6861431/xxlarge1087.gif) ![rcy](/content/x7764372l6861431/xxlarge1088.gif) ![icy](/content/x7764372l6861431/xxlarge1080.gif) ![mcy](/content/x7764372l6861431/xxlarge1084.gif) ![iecy](/content/x7764372l6861431/xxlarge1077.gif) ![rcy](/content/x7764372l6861431/xxlarge1088.gif) ![scy](/content/x7764372l6861431/xxlarge1089.gif) ![ocy](/content/x7764372l6861431/xxlarge1086.gif) ![lcy](/content/x7764372l6861431/xxlarge1083.gif) ![iecy](/content/x7764372l6861431/xxlarge1077.gif) Na2SO4·10H2O, CH3COONa·3H2O, Na2S·5H2O, Na2S·9H2O, Mg(NO3)2·6H2O, MgCl2·6H2O ![ecy](/content/x7764372l6861431/xxlarge1101.gif) ![vcy](/content/x7764372l6861431/xxlarge1074.gif) ![tcy](/content/x7764372l6861431/xxlarge1090.gif) ![iecy](/content/x7764372l6861431/xxlarge1077.gif) ![kcy](/content/x7764372l6861431/xxlarge1082.gif) ![tcy](/content/x7764372l6861431/xxlarge1090.gif) ![icy](/content/x7764372l6861431/xxlarge1080.gif) ![chcy](/content/x7764372l6861431/xxlarge1095.gif) ![iecy](/content/x7764372l6861431/xxlarge1077.gif) ![scy](/content/x7764372l6861431/xxlarge1089.gif) ![kcy](/content/x7764372l6861431/xxlarge1082.gif) ![ocy](/content/x7764372l6861431/xxlarge1086.gif) ![scy](/content/x7764372l6861431/xxlarge1089.gif) ![mcy](/content/x7764372l6861431/xxlarge1084.gif) ![iecy](/content/x7764372l6861431/xxlarge1077.gif) ![scy](/content/x7764372l6861431/xxlarge1089.gif) Mg(NO3)2·6H2O·MgCl2·6H2O.
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