Synthesis and crystal structure of nickel(II) complex based on 2-trifluoroacetylcycloalkanone benzoylhydrazones |
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Authors: | B B Umarov K G Avezov M A Tursunov N G Sevinchov N A Parpiev G G Aleksandrov |
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Institution: | 1. Bukhara State University, Bukhara, 705018, Uzbekistan 2. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 117907, Russia
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Abstract: | The reaction of ethanol solutions of benzoylhydrazones of 2-trifluoroacetylcycloalkanones (H2L) with a solution of nickel(II) acetate in aqueous ammonia in 1 : 1 ratio gave complexes NiL · NH3 with square structure. The composition and structure of the complexes were determined by elemental analysis, IR and 1H NMR spectroscopy, and X-ray diffraction analysis. |
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