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Preparation,Separation and Identification of Partially Methylated Alditol Acetates for use as Standards in Methylation Analysis
Authors:Elisabeth T Oakley  Donald F Magin  Gordon H Bokelman  William S Ryan Jr
Institution:Philip Morris, U.S.A. Research and Development , P. O. Box 26583, Richmond, VA, 23251
Abstract:A procedure is described for a simple preparation that produces mixtures of a majority of the possible O-methylated alditol acetate derivatives of neutral monosaccharides. The derivatives can be used as standards to determine both the linkage positions and the precise identities of sugar constituents in cell wall poly-saccharides.
Keywords:Synthesis  Tetrasaccharide  Enterohemorrhagic Escherichia coli type O157
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