Effective Route to Graphitic carbon Nitride from Ball-Milled Amorphous carbon in NH3 Atmosphere Under Annealing |
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作者姓名: | 费振义 刘玉先 |
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作者单位: | CollegeofMaterialsScienceandEngineering,ShandongUniversity,Ji‘nan250061 |
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摘 要: | Graphitic carbon nitride (g-C3N4) powders were successfully synthesized from ball-milled amorphous carbon under NH3 atmosphere at high temperature, for the first time to the best of our knowledge. The combined charac-teristic data obtained by x-ray diffraction, high-resolution transmission-electron microscopy, electron energy losss pectroscopy, Raman spectroscopy, energy dispersive spectroscopic analysis, and Fourier transformation infrared spectroscopy provide substantial evidence for the graphite-like sp^2-bonded structure with C3N4 stoichiometry.
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关 键 词: | 碳氮化物 NH3 氨气气氛 退火 球磨石墨粉 非晶态碳 合成 拉曼光谱 X射线衍射 傅里叶变换 能谱分析 |
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