Di(adamant-1-yl)- and di(adamant-2-yl)thiophosphoric acids and their triethylammonium salts in alkylation reactions |
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Authors: | R I Yurchenko Yu M Klimko A A Esipenko E D Butova A G Yurchenko |
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Institution: | 1.Kiev Polytechnic Institute,National Technical University of Ukraine,Kiev,Ukraine |
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Abstract: | By reaction of di(adamant-1-yl) and di(adamant-2-yl) phosphites with sulfur in the presence of triethylamine diadamantylthiophosphoric
acid triethylammonium salts were obtained. The latter by the action of hydrochloric acid were converted into free thiophosphoric
acids and by the reaction of alkylation into the respective triesters which have thionic structure. Applicability in such
reactions also of triethylammonium salts of diadamantyldithiophosphoric acids was demonstrated. |
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