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Use of Passive and Grab Sampling and High-Resolution Mass Spectrometry for Non-Targeted Analysis of Emerging Contaminants and Their Semi-Quantification in Water
Authors:&#x;or&#x;e Tadi&#x;  Rayana Manasfi  Marine Bertrand  Andrs Sauvêtre  Serge Chiron
Institution:1.Hydrosciences Montpellier, University Montpellier, CNRS, IRD, 34090 Montpellier, France; (R.M.); (S.C.);2.Hydrosciences Montpellier, University Montpellier, IMT Mines Ales, CNRS, IRD, 30100 Ales, France; (M.B.); (A.S.)
Abstract:Different groups of organic micropollutants including pharmaceuticals and pesticides have emerged in the environment in the last years, resulting in a rise in environmental and human health risks. In order to face up and evaluate these risks, there is an increasing need to assess their occurrence in the environment. Therefore, many studies in the past couple of decades were focused on the improvements in organic micropollutants’ extraction efficiency from the different environmental matrices, as well as their mass spectrometry detection parameters and acquisition modes. This paper presents different sampling methodologies and high-resolution mass spectrometry-based non-target screening workflows for the identification of pharmaceuticals, pesticides, and their transformation products in different kinds of water (domestic wastewater and river water). Identification confidence was increased including retention time prediction in the workflow. The applied methodology, using a passive sampling technique, allowed for the identification of 85 and 47 contaminants in the wastewater effluent and river water, respectively. Finally, contaminants’ prioritization was performed through semi-quantification in grab samples as a fundamental step for monitoring schemes.
Keywords:non-target screening  passive sampling  contaminants of emerging concern  transformation products  wastewater  river water  semi-quantification
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