9-H-9-Borafluorene dimethyl sulfide adduct: a product of a unique ring-contraction reaction and a useful hydroboration reagent |
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| Authors: | Das Animesh Hübner Alexander Weber Mitra Bolte Michael Lerner Hans-Wolfram Wagner Matthias |
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| Affiliation: | Institut für Anorganische Chemie, Goethe-Universit?t Frankfurt, Max-von-Laue-Strasse 7, D-60438 Frankfurt (Main), Germany. |
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| Abstract: | The dimethyl sulfide adduct 2(DMS) is a crystalline storage form of the unstable hydroboration reagent 9-H-9-borafluorene (2); 2(DMS) is available by the addition of DMS to either in situ generated [2](2) or 1,2-(2,2'-biphenylylene)diborane(6) (7). |
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