Synthesis of phosphorus-containing polyoxamacrocycles with one to two reactive thiophosphoryl chloride groups |
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| Authors: | Xiao Mei Zhang Dao Quan Wang Wan Yi Chen |
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| Institution: | a Department of Applied Chemistry, China Agricultural University, Beijing 100094, China;b College of Chemical Engineering, Anhui University of Science and Technology, Huainan 232001, China |
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| Abstract: | Novel phosphorus-containing polyoxamacrocycles with one to two reactive thiophosphoryl chloride groups 5, 6, 7, 8 were synthesized from bishydroxyl compounds 1, 2, 3, 4 and thiophosphoryl chloride respectively. Their structures were confirmed by 1H NMR, 13C NMR, 31P NMR and elemental analysis. |
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| Keywords: | Phosphorus-containing macrocycle Phosphorus-containing polyoxamacrocycle Thiophosphoryl chloride cyclization |
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