Synthesis of 3, 6-anhydrocellulose by the saponification of 6-O-tosyl-2, 3-di-O-acetylcellulose |
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Authors: | Yu M Makhsudov L G Krylova L S Gal'braikh and A Z Rogovin |
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Institution: | (1) Moscow Textile Institute, USSR |
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Abstract: | Summary 1. Derivatives of cellulose containing 3, 6-anhydro rings have been synthesized by the following route: cellulose 6-O-tritylcellulose 6-O-trityl-2, 3-di-O-acetylcellulose 2, 3-di-O-acetylcellulose 6-O-tosyl-2, 3-di-O-acetylcellulose 3, 6-anhydrocellulose.2. The composition of the 3, 6-anhydrocellulose has been studied by exhaustive acetylation, nitration, and periodate oxidation, and also by IR spectroscopy.Khimiya Prirodnykh Soedinenii, Vol. 2, No. 6, pp. 372–375, 1966 |
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