Electrodeposition of milligram amounts of uranium on electropolished stainless steel disks |
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Authors: | S. K. Aggarwal P. M. Shah R. K. Duggal H. C. Jain |
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Affiliation: | (1) Fuel Chemistry Division, Bhabha Atomic Research Center, Trombay, 400 085 Bombay, India |
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Abstract: | Investigations have been carried out for the electrodeposition of milligram amounts of uranium on electropolished stainless steel disks with an objective of preparing good quality sources for -spectrometric studies on uranium. The parameters studied include the variation of electrodeposition yield as a function of voltage, time, distance between the cathode and anode, and the volume of 0.2M ammonium oxalate solution. The conditions selected for preparing good quality sources with nearly 100% yield were: electrodeposition voltage 25 V, time of deposition 15 min, volume of 0.2M ammonium oxalate solution in the cell 4 ml and a distance of 2 cm between the cathode and anode. The sources prepared using this method have been used successfully for the -spectrometric determination of234U/238U ratios in uranium samples. |
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