Matrix Solid-phase Dispersion Extraction of Alkaloids from the Roots of Aconitum kusnezoffii Reichb |
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Authors: | WEI Wei LI Xu-wen SHI Xiao-lei ZHOU Hong-yu YANG Rui-jie ZHANG Han-qi JIN Yong-ri College of Chemistry Jilin University Changchun P. R. China |
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Affiliation: | WEI Wei,LI Xu-wen,SHI Xiao-lei,ZHOU Hong-yu,YANG Rui-jie,ZHANG Han-qi and JIN Yong-ri College of Chemistry,Jilin University,Changchun 130012,P. R. China |
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Abstract: | Matrix solid-phase dispersion(MSPD) was developed for the extraction of four alkaloids, including aconitine, mesaconitine, hypaconitine and deoxyaconitine, from the roots of Aconitum kusnezoffii Reichb. The determination of the analyte was carried out by high performance liquid chromatography with UV detection. The alkaline alumina was used as sorbent. The mixture of acetonitrile and water was used as elution solvent. Several extraction parameters, such as type of sorbent, the ratio of sample to solid suppo... |
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Keywords: | Matrix solid-phase dispersion Aconitine-type alkaloid Aconitum kusnezoffii Reichb. Extraction High-performance liquid chromatography |
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