Abstract: | In this study, a number of new diheterocyclic thioureas have been synthesized under microwave irradiation coupled with solvent‐free condition, which proves to be simple and efficient. The structures of the prepared compounds are characterized by elemental analysis, IR, 1H NMR, and 13C NMR spectra. © 2006 Wiley Periodicals, Inc. Heteroatom Chem 17:148–151, 2006; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/hc.20193 |