Ultrasound-promoted tosylation of oligo(ethylene glycols) |
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Authors: | Danjou Pierre-Edouard Wallyn Damien Cazier-Dennin Francine Delattre François |
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Affiliation: | Univ. Lille Nord de France, F-5900 Lille, France. |
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Abstract: | A series of oligo(ethylene glycols) was efficiently tosylated by ultrasound procedure within dichloromethane in the presence of triethylamine. Results show that sonochemical synthesis of oligo(ethylene glycol) ditosylates has a double advantage since it does not use catalysts and it drastically reduces the reaction time. This straightforward method represents an eco-friendly alternative to the traditional tosylation by pyridine synthesis. |
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