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Synthesis and characterization of MgF2 and KMgF3 nanorods
Authors:Minhua Cao  Yanjuan Qi  Changwen Hu
Affiliation:
  • a Faculty of Chemistry, Institute of Polyoxometalate Chemistry, Northeast Normal University, Changchun 130024, PR China
  • b Department of Chemistry, Beijing Institute of Technology, Beijing 100081, PR China
  • Abstract:MgF2 nanorods with diameters of 60-100 nm were synthesized by a microemulsion method. Subsequent hydrothermal reaction of as-synthesized MgF2 nanorods and KF at 240°C for 3 days or 140°C for 7 days resulted in KMgF3 nanorods, which retained the rod-like morphology of the source material MgF2 in the reaction process. The morphology of as-synthesized MgF2 strongly depended on the molar ratio between water and the surfactant CTAB and the concentration of CTAB.
    Keywords:One-dimensional nanostructures   MgF2   KMgF3   Microemulsion   Hydrothermal reactions
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