| Crystal Structure of Bis(3-hydroxy-2-pyridyl)disulfide |
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| 引用本文： | 陈学太,胡永韩,等. Crystal Structure of Bis(3-hydroxy-2-pyridyl)disulfide[J]. 结构化学, 1994, 13(2): 155-158 |
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| 作者姓名： | 陈学太 胡永韩 等 |
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| 作者单位： | State Key Laboratory of Structural Chemistry and Fujian Institute of Research on the Structure of Matter，Chinese Academy of Sciences，Fuzhou，Fujian 350002 |
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| 摘 要： | ＣｒｙｓｔａｌＳｔｒｕｃｔｕｒｅｏｆＢｉｓ（３－ｈｙｄｒｏｘｙ－２－ｐｙｒｉｄｙｌ）ｄｉｓｕｌｆｉｄｅＣｈｅｎＸｕｅ－Ｔａｉ；ＫａｎｇＢｅｉ－Ｓｈｅｎｇ；ＸｕＹｏｎｇ－Ｊｉｎ；ＨｕＹｏｎｇ－Ｈａｎ（ＳｔａｔｅＫｅｙＬａｂｏｒａｔｏｒｙｏｆＳｔｒｕｃｔ...
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| 关 键 词： | 晶体结构 合成 双（3－羟基－2－吡啶基）二硫醚 |
Crystal Structure of Bis(3-hydroxy-2-pyridyl) disulfide |
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| Chen Xue-Tai,Kang Bei-Sheng,Xu Yong-Jin,Hu Yong-Han. Crystal Structure of Bis(3-hydroxy-2-pyridyl) disulfide[J]. Chinese Journal of Structural Chemistry, 1994, 13(2): 155-158 |
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| Authors: | Chen Xue-Tai Kang Bei-Sheng Xu Yong-Jin Hu Yong-Han |
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| Affiliation: | [1]StateKeyLaboraoryofStructuralChemistryandFujianIns [2]StateKeyLaboraoryofStructural |
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| Abstract: | C_(10)H_8N_2O_2S_2, Mr=252. 32,monoclinic,P2_(1/c),a=7.165(5).b=7.659(3),c=19.543(8)A,β=96. 76(5)°,V=1065.0(9) A,Z=4,D_c=1. 57 g/cm￣3.The structure was solved by direct methods and refined to final R(R_w)=0.051(0.057) for 1446 observed reflections with I≥3σ(Ⅰ).The sulfur-sulfur bond length is found to be 2. 019(2) A with a dihedral angle CSSC of 93.29°. |
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| Keywords: | Crystal structure synthesis disulfide |
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