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原子荧光光谱法快速测定粉煤灰中砷与汞
引用本文:祝建国,毛振才,毛恺霞,武学军,王玉功.原子荧光光谱法快速测定粉煤灰中砷与汞[J].分析测试技术与仪器,2007,13(3):219-221.
作者姓名:祝建国  毛振才  毛恺霞  武学军  王玉功
作者单位:1. 国土资源部,兰州矿产资源监督检测中心,甘肃,兰州,730050
2. 国土资源部,兰州矿产资源监督检测中心,甘肃,兰州,730050;甘肃国电龙源洁净燃烧工程技术有限责任公司,甘肃,兰州,730050
3. 甘肃国电龙源洁净燃烧工程技术有限责任公司,甘肃,兰州,730050
摘    要:采用王水分解试样-原子荧光光谱法(AFS)测定粉煤灰中的砷、汞,方法回收率分别为98.5%~102.0%、85.0%~105.0%,相对偏差分别为1.9%~4.8%、0.6%~2.4%.方法具有快速、简便、灵敏等优点,对探讨粉煤灰在农业生态环境方面的综合利用颇有价值.

关 键 词:原子荧光光谱法  粉煤灰    
文章编号:1006-3757(2007)03-0219-03
收稿时间:2007-04-10
修稿时间:2007-05-21

Rapid Determination of Arsenic and Mercury in Coal Fly Ash by Atomic Fluorescence Spectrometry
ZHU Jian-guo,MAO Zhen-cai,MAO Kai-xi,WU Xue-jun and WANG Yu-gong.Rapid Determination of Arsenic and Mercury in Coal Fly Ash by Atomic Fluorescence Spectrometry[J].Analysis and Testing Technology and Instruments,2007,13(3):219-221.
Authors:ZHU Jian-guo  MAO Zhen-cai  MAO Kai-xi  WU Xue-jun and WANG Yu-gong
Institution:1. Lanzhou Center of Product Quality Supervision Inspection of National Land and Natural Resources, Lanzhou 730050, China ;2. Gansu SP Longyuan Clean Combustion Engineering Technology Co LTD, Lanzhou 730050,China
Abstract:The sample was dissolved in aqua vegia; AFS method was used to determine arsenic and mercury in coal fly ash. The ralative stand deviations of them are 1.9%-4.8%,0. 6%-2.4%. The recovery of them is 98. 5% - 102. 0%, 85. 0% - 105. 0% respectively. The method is simple, quick and high sensitivity. The method has been applied to comprehensive utilization of coal fly ash in monitor agriculture ecology environment.
Keywords:atomic fluorescence spectrometry  coal fly ash  arsenic  mercury  
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