Facile solvent-free synthesis and structural elucidation of styrylcyclohex-2-enone derivatives |
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| Authors: | Mohammad M Mojtahedi Mohammad Saeed Abaee Mohammad Mehdi Zahedi Mohammad R Jalali A Wahid Mesbah Werner Massa Roholah Yaghoubi Mehdi Forouzani |
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| Institution: | (1) Organic Chemistry Laboratory, Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran;(2) Fachbereich Chemie der Philipps-Universitaet Marburg, Marburg, Germany;(3) Sari Center, Payam Noor University, Sari, Iran |
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| Abstract: | A remarkably efficient procedure for the synthesis of styrylcyclohex-2-enone derivatives at room temperature is described
using a mild reaction medium consisting of lithium perchlorate and N-(trimethylsilyl)diethylamine. Several compounds of this class are synthesized conveniently and rapidly. Spectroscopic and
X-ray diffraction experiments confirm the proposed structures.
Correspondence: Mohammad M. Mojtahedi and Mohammad Saeed Abaee, Organic Chemistry Laboratory, Chemistry and Chemical Engineering
Research Center of Iran, P.O. Box 14335-186, Tehran, Iran. |
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| Keywords: | Claisen-Schmidt condensation α β -Unsaturated carbonyls Solvent-free Lithium perchlorate |
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