The catalysis, synthesis and characterization of ferrocenylchalcone |
| |
| Authors: | Yu-Ting Liu Li Feng Da-Wei Yin |
| |
| Institution: | 1. Key Laboratory of Auxiliary Chemistry & Technology for Chemical Industry, Ministry of Education, Shaanxi University of Science & Technology, Xi’an, 710021, China
2. School of Chemistry and Chemical Engineering, Shaanxi University of Science & Technology, Xi’an, 710021, China
|
| |
| Abstract: | Eight kinds of ferrocenylchalcone derivatives were synthesized by the reaction of acetylferrocene and aromatic aldehyde using solid as catalyst in the experiment. The influrence of the catalysts, the raw material molar ratios and reaction times on the yield of ferrocenylchalcone derivatives are discussed. The optimal conditions of synthesis reaction have been selected: the catalyst was KF/Al2O3, n(acetyl ferrocene)/n(formal dehyde) = 1:1.2. The structures of the products were characterized by melting point test, IR, 1HNMR, 13CNMR and elemental analysis. |
| |
| Keywords: | |
| 本文献已被 SpringerLink 等数据库收录！ |
|
