| 酸性离子液体[Hnmp]HSO4催化下一锅三组分反应合成N-(2-羟基-1-萘基)(苯基)甲基-吡咯烷-2-酮衍生物 |
| |
| 引用本文： | 田金金,郭红云,邵鸿斌. 酸性离子液体[Hnmp]HSO4催化下一锅三组分反应合成N-(2-羟基-1-萘基)(苯基)甲基-吡咯烷-2-酮衍生物[J]. 有机化学, 2011, 31(11) |
| |
| 作者姓名： | 田金金 郭红云 邵鸿斌 |
| |
| 作者单位： | 浙江工业大学化学工程与材料学院 杭州310014 |
| |
| 摘 要： | 在无溶剂条件下,利用廉价无毒的酸性离子液体[Hnmp]HSO4为催化剂,醛、2-萘酚和吡咯烷酮一锅三组分合成了一系列新颖的N-(2-羟基-1-萘基)(苯基)甲基-吡咯烷-2-酮衍生物.与现有的方法相比该方法避免使用有机溶剂,且反应时间短,产率高,离子液体廉价易制备,且可回收重复再利用.
|
| 关 键 词： | 酸性离子液体 2-萘酚 吡咯烷酮 N-(2-羟基-1-萘基)(苯基)甲基-吡咯烷-2-酮衍生物 |
One-Pot Three-Component Synthesis of N-(2-Hydroxynaphthalen-1-yl)(phenyl)methyl-pyrrolidin-2-ones Catalyzed by Acidic Ionic Liquid [Hnmp]HSO4 |
| |
| Tian, Jinjin,Guo, Hongyun,Shao, Hongbin. One-Pot Three-Component Synthesis of N-(2-Hydroxynaphthalen-1-yl)(phenyl)methyl-pyrrolidin-2-ones Catalyzed by Acidic Ionic Liquid [Hnmp]HSO4[J]. Chinese Journal of Organic Chemistry, 2011, 31(11) |
| |
| Authors: | Tian Jinjin Guo Hongyun Shao Hongbin |
| |
| Affiliation: | Tian,Jinjin Guo,Hongyun Shao,Hongbin(College of Chemical Engineering and Material Science,Zhejiang University of Technology,Hangzhou 310014) |
| |
| Abstract: | A series of novel N-(2-hydroxynaphthalen-1-yl)(phenyl)methyl-pyrrolidin-2-ones were synthesized employing a one-pot three-component condensation reaction of aromatic aldehydes,2-naphthol and pyr-rolidin-2-one catalyzed by HSO4 under solvent-free conditions.This method does not involve any haz-ardous organic solvent and has the advantages of short reaction time,high yields compared with the reported methods.Moreover,the ionic liquid is easy to prepared and could be recycled for subsequent reactions. |
| |
| Keywords: | acidic ionic liquid 2-naphthol pyrrolidin-2-one N-(2-hydroxynaphthalen-1-yl)(phenyl)-methyl-pyrrolidin-2-one |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
