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Isolation of oxygen-containing monoterpenoids of essential oils by preparative adsorption chromatography with gradient elution
Authors:S. V. Sur
Abstract:A simple and effective procedure for the comparative chromatography of 1–2 ml of essential oils on a 40×250 mm column of silica gel with gradient elution by hexane-diethyl ether has been developed. A simple system of preparing the mobile phase permits the creation of a continuous gradient during chromatography. The efficacy of the procedure has been shown taking as an example the isolation of fenchone from fennel essential oil. A. V. Dumanskii Institute of Colloid Chemistry and the Chemistry of Water, Ukrainian Academy of Sciences, Kiev. Translated from Khimiya Prirodnykh Soedinenii, No. 5, pp. 634–637, September–October, 1991.
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