Synthesis of titanium sulfides under high pressure |
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| Affiliation: | 1. Department of Energy Conversion and Storage, Faculty of Chemistry, Gdańsk University of Technology, Narutowicza 11/12, Gdańsk 80-233, Poland;2. Fachbereich Material und Geowissenschaften, Technische Universität Darmstadt, Otto-Berndt-Straße 3, Darmstadt 64287, Germany;3. Faculty of Chemistry, Nicolaus Copernicus University in Toruń, Gagarina 7, Toruń 87-100, Poland |
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| Abstract: | Titanium sulfides were synthesized in the temperature range 600–750°C and in the pressure range 10–200 MPa with an apparatus used for hydrothermal synthesis. Stoichiometric TiS2 cannot be prepared under atmospheric pressure, but was synthesized under high pressure. Also the phase relationship between TiS2 and TiS3 has been established under high pressure up to 200 MPa, and the pressure-temperature phase diagram for TiS system is presented. |
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