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Preparation of LiCoO2 nanofibers by electrospinning technique
Authors:Changlu Shao  Na Yu  Rixiang Mu
Affiliation:a Center for Advanced Optoelectronic Functional Materials Research, Northeast Normal University, Changchun 130024, China
b Nanoscale Materials and Sensors, Department of Physics, Fisk University, Nashville, TN, USA
Abstract:Using a sol-gel processing and electrospinning technique, extrathin fibers of PVA (polyvinyl alcohol)/lithium chloride/cobalt acetate composite were prepared. After calcinations of the above precursor fibers at 600°C, LiCoO2 nanofibers with a diameter of 100-150 nm, were successfully obtained. Measurements of TG/DTA, IR, XRD, Raman, SEM, EDS, respectively, were performed to characterize the properties of the as-prepared materials. We observed a strong correlation between crystalline phase and morphology of the fibers and calcinations temperature.
Keywords:A. Oxides   C. X-ray diffraction
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