| 3-N-丙酰基-2-芳基-5-(2-碘苯基)-1,3,4-噁唑啉类化合物的合成 |
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| 引用本文： | 毕秀成,李德江,傅和青.3-N-丙酰基-2-芳基-5-(2-碘苯基)-1,3,4-噁唑啉类化合物的合成[J].合成化学,2007,15(4):484-486,490. |
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| 作者姓名： | 毕秀成 李德江 傅和青 |
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| 作者单位： | 1. 郧阳师范专科学校,化学系,湖北,丹江口,442700
2. 华南理工大学,化工研究所,广东,广州,510640 |
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| 摘 要： | 2-碘苯甲酰肼与芳醛反应得到相应的酰腙(1),1再与丙酸酐脱水环化合成了3-N-丙酰基-2-芳基-5-(2-碘苯基)-1,3,4-噁唑啉类化合物,其结构经1H NMR,IR,MS和元素分析表征。
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| 关 键 词： | 苯酰肼 苯甲酰腙 噁唑啉 合成 |
| 文章编号： | 1005-1511（2007）04-0484-03 |
| 收稿时间： | 2006-11-24 |
| 修稿时间： | 2006-11-24 |
Synthesis of 3-N-propanoyl-2-aryl-5-(2-iodophenyl)-1,3,4-oxadiazolines |
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| BI Xiu-cheng,LI De-jiang,FU He-qing.Synthesis of 3-N-propanoyl-2-aryl-5-(2-iodophenyl)-1,3,4-oxadiazolines[J].Chinese Journal of Synthetic Chemistry,2007,15(4):484-486,490. |
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| Authors: | BI Xiu-cheng LI De-jiang FU He-qing |
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| Institution: | 1. Department of Chemistry, Yunyang Normal College, Danjiangkou 442700, China; 2. Institute of Chemical Engineering, South China University of Technology, Guangzhou 510640, Chian |
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| Abstract: | 3-N-Propanoyl-2-aryl-5-(2-iodophenyl)-1,3,4-oxadiazolines were synthesized by cyclization between propanoic anhydride and hydrazones from 2-iodobenzoyl hydrazin and arylaldehydes.The structures were confirmed by 1H NMR,IR,MS and elemental analysis. |
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| Keywords: | benzoyl hydrazine benzoyl hydrazone oxazoline synthesis |
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