Die Kristallstruktur von [Cl4P{i-Prop-NC(Cl)N-i-Prop}]

Crystal Structure of [Cl₄P{i-Prop-NC(Cl)N-i-Prop}] The monomeric di-isopropylcarbodiimide complex [Cl₄P{i-Prop-NC(Cl)N-i-Prop}] crystallizes in the monoclinic space group C2 with 4 formula units in the unit cell and with the lattice constants a = 1391.2(2), b = 708.6(1), c = 1463.5(2) pm and β = 95.76(1)°. The structure was refined to an R-value of 0.026 (2084 independent, observed reflexions). Main parts of the IR and Raman spectrum of the compound are discussed.