Reaction of trialkyl-(3-aminopropyl)silanes with formaldehyde and elemental sulfur |
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| Authors: | N. N. Vlasova A. E. Pestunovich V. A. Pestunovich V. V. Keiko T. K. Pogodaeva M. G. Voronkov |
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| Affiliation: | (1) Irkutsk Institute of Organic Chemistry, Siberian Branch of the Academy of Sciences of the USSR, USSR |
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| Abstract: | Conclusions N-(3-Trialkylsilylpropyl)formamides (II) and N,N -bis(3-trialkylsilylpropyl)thioureas (III), together with a small amount of the trialkyl-(3-isothiocyanatopropyl)silane, are formed when trialkyl-(3-aminopropyl)silanes are reacted with formaldehyde and sulfur in aqueous-ethanol medium. 1,3,5-Tris(trialkylsilylpropyl)hexahydrotriazines are the intermediate products in these reactions.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 666–668, March, 1977. |
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