| 安息香的常规、半常量及微型制备方法的比较与评估 |
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| 引用本文： | 夏小庆,黄勤安,吴运军,方骏. 安息香的常规、半常量及微型制备方法的比较与评估[J]. 实验室科学, 2013, 16(3): 38-39,42 |
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| 作者姓名： | 夏小庆 黄勤安 吴运军 方骏 |
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| 作者单位： | 皖南医学院化学教研室,安徽芜湖,241002 |
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| 基金项目： | 皖南医学院教研项目"绿色化学实验室的建设研究" |
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| 摘 要： | 为了研究在常规条件下开展小量化实验的可行性,分别按常规、半常量及微型三种方式对安息香的制备方法进行对比实验,结果表明,半常量法优于常规法和微型法。在pH为8-9及适量锌粉存在下,安息香的半常量合成节约实验经费、缩短实验时间、减少污染,有效地提高了实验效率。
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| 关 键 词： | 常规实验 半常量实验 微型实验 安息香 维生素B1 |
Comparison and evaluation of routine, semi-micro and microscale preparation method of benzoin |
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| XIA Xiao-qing , HUANG Qin-an , WU Yun-jun , FANG Jun. Comparison and evaluation of routine, semi-micro and microscale preparation method of benzoin[J]. Laboratory Science, 2013, 16(3): 38-39,42 |
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| Authors: | XIA Xiao-qing HUANG Qin-an WU Yun-jun FANG Jun |
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| Affiliation: | (Department of Chemistry, Wannan Medical College, Wuhu 241002, China) |
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| Abstract: | To study the feasibility of conducting small- sized experiment in common experiment conditions, the three different processes of producing Benzoin, namely the routine, semi- routine and microscale experiments are compared and evaluated. The results indicate semi- routine experiment method is superior to the routine and microscale ones. When pH is 8-9 and some zinc powder exists, the semi-routine chemical synthesizing of benzoin can save experimental funding, shorten the reaction time and reduce pollution. So the efficiency has been greatly improved. |
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| Keywords: | routine experiment semiroutine experiment microscale experiment benzoin vitamin B1 |
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