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极谱法测定矿石中高含量钨
引用本文:梁云生,毛禹平.极谱法测定矿石中高含量钨[J].中国无机分析化学,2013,3(2):32-34.
作者姓名:梁云生  毛禹平
作者单位:昆明冶金研究院,云南省选冶新技术重点实验室,云南 昆明 650031;昆明冶金研究院,云南省选冶新技术重点实验室,云南 昆明 650031
摘    要:提出了用JP-303型智能化极谱仪,测定≥1%以上钨的极谱分析法。拟定方法与现行采用的"硫氰酸盐"分光光度法相比,有着测定范围宽(WO3含量在X%~XX%),快速、简便、准确的优点。方法的标准曲线相关系数0.999,样品加标回收率为98.4%~101.4%,可用于WO3的选冶生产控制分析,效果良好。

关 键 词:极谱法  测定  矿石  高含量钨
收稿时间:2013/1/25 0:00:00
修稿时间:2013/3/16 0:00:00

Determination of High Tungsten Content in the Ore by Polarograph
LIANG Yunsheng and MAO Yuping.Determination of High Tungsten Content in the Ore by Polarograph[J].Chinese Journal of Inorganic Analytical Chemistry,2013,3(2):32-34.
Authors:LIANG Yunsheng and MAO Yuping
Institution:(Kunming Metallurgy Research Institute ,Yunnan Key Laboratory for New Technology of Beneficiation and Metallurgy Kunming ,Yunnan 650031 ,China)
Abstract:his paper proposed an analysis method for using a Jp-303 type Intelligent Polarograph to determine high tungsten content (higher than 1%) in the ore. Comparing with conventional thiocyanate spectrophotometric method , the proposed method is faster, easier, more accurate and has wider analysis range (the content of WO~ can be from XQ/'~0 to XX% ). The correlation coefficient of the calibration curve is over 0. 999. The standard addition recovery is 98.4%. This method can be used for production control analysis in beneficiation and metallurgy industry with satifictory results.
Keywords:Polarograph analysis method  determination  ore  high tungsten content
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