College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou 310014, China
Abstract:
Gibberellin A4 is effectively separated from mixture of gibberellin A4 and its analugue gibberellin A7, in the form of its crystalline complex with N,N,N',N'-tetramethylethylenediamine. After removing the tetramethylethylenediamine from the crystal by dilute HCl, gibberellin A4 is obtained a purity of 98.1% and a yield of 72.7%.