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Synthesen und Kristallstrukturen von [(t-Bu4Sb4)Fe(CO)4], [(t-Bu4Sb4)Mo(CO)5] und [(t-Bu3Sb4)Mo(η5-C5Me5)(CO)3] |
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| Authors: | H J Breunig R Rsler E Lork |
| Abstract: | Syntheses and Crystal Structures of ( t -Bu4Sb4)Fe(CO)4], ( t -Bu4Sb4)Mo(CO)5], and ( t -Bu3Sb4)Mo(η5-C5Me5)(CO)3] t-Bu4Sb4 reacts with Fe2(CO)9 to form (t-Bu4Sb4)Fe(CO)4] ( 1 ). (t-Bu4Sb4)Mo(CO)5] ( 2 ) is formed from (thf)Mo(CO)5 and t-Bu4Sb4. (t-Bu3Sb4)Mo(η5-C5Me5)(CO)3] ( 3 ) is a product of the reaction of t-Bu4Sb4 with (η5-C5Me5)Mo(CO)3]2. The crystal structures of 1–3 are reported. |
| Keywords: | Antimony Iron complex Molybdenum complex X-ray diffraction |