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γ-Al2O3柔性纳米纤维膜的制备及机械性能
引用本文:李微,赵晓敏,王延风,路文娟,贾玉娜,焦秀玲,陈代荣,张平平.γ-Al2O3柔性纳米纤维膜的制备及机械性能[J].高等学校化学学报,2017,38(6):915.
作者姓名:李微  赵晓敏  王延风  路文娟  贾玉娜  焦秀玲  陈代荣  张平平
作者单位:1. 山东大学化学与化工学院, 济南 2501002. 山东大学生命科学学院, 济南 2501003. 山东省医学科学院药物研究所, 济南 2500624. 国家胶体材料工程技术研究中心, 济南 250100
基金项目:山东省医学科学院医药卫生科技创新工程、 国家自然科学基金(批准号: 21305079)和山东省自然科学基金(批准号: ZR2015YL040)资助.
摘    要:以氯化铝和异丙醇铝为原料, 水和乙醇为溶剂, 通过溶胶凝胶结合静电纺丝法制备了柔性γ-Al2O3纳米纤维膜. 表征了纤维膜的形貌和机械性质, 并研究了纤维膜的形成过程. 组成纤维膜的纤维直径均匀, 平均直径188 nm, 纤维由粒径在15~30 nm的纳米颗粒组成且表面光滑. 制备的纤维膜具有较好的柔性及抗拉强度(1.01 MPa).

关 键 词:Al2O3  纤维膜  机械性质  静电纺丝  
收稿时间:2016-11-29

Fabrication and Mechanical Properties of Flexible γ-Al2O3 Nanofibrous Membranes
LI Wei,ZHAO Xiaomin,WANG Yanfeng,LU Wenjuan,JIA Yuna,JIAO Xiuling,CHEN Dairong,ZHANG Pingping.Fabrication and Mechanical Properties of Flexible γ-Al2O3 Nanofibrous Membranes[J].Chemical Research In Chinese Universities,2017,38(6):915.
Authors:LI Wei  ZHAO Xiaomin  WANG Yanfeng  LU Wenjuan  JIA Yuna  JIAO Xiuling  CHEN Dairong  ZHANG Pingping
Institution:1. School of Chemistry & Chemical Engineering, Shandong University, Jinan 250100, China;2. School of Life Sciences, Shandong University, Jinan 250100, China3. Institute of Materia Medica, Shandong Academy of Medical Sciences, Jinan 250062, China4. National Engineering Research Center for Colloidal Materials, Shandong University, Jinan 250100, China
Abstract:Flexible γ-Al2O3 nanofibrous membranes were prepared by sol-gel combined electrospinning technique using aluminum chloride and aluminum isopropoxide as raw materials, water and ethanol as the solvents. The morphology and mechanical property of the membranes were characterized and the formation process was tracked. The membranes were composed of uniform nanofibers with a mean diameter of ca.188 nm. The fibers’ surfaces were smooth and the fibers were composed of nanoparticles with a size range of 15—30 nm. The prepared membranes exhibited excellent flexibility and tensile strength(1.01 MPa).
Keywords:Al2O3  Fibrous membrane  Mechanical property  Electrospinning  
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