| 杀虫剂呋喃虫酰肼的高效液相色谱分析 |
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| 引用本文： | 聂果,吴春先,高立明,王广成,陈丙坤,张忠明.杀虫剂呋喃虫酰肼的高效液相色谱分析[J].西南师范大学学报(自然科学版),2009,34(6). |
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| 作者姓名： | 聂果 吴春先 高立明 王广成 陈丙坤 张忠明 |
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| 作者单位： | 四川省农药检定所,成都,610041 |
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| 摘 要： | 采用反相高效液相色谱法对呋喃虫酰肼进行定量分析.反相高效液相色谱条件:使用C18反相柱和二极管阵列检测器.以V(甲醇)+V(水)=70+30为流动相,柱温30℃,流速:1.0 mL/min,检测波长202 nm,外标法对呋喃虫酰肼的有效成分进行定量分析.结果表明呋喃虫酰肼的线性关系系数R为0.999 9,测定10%呋喃虫酰肼悬浮剂时,标准偏差为0.14,变异系数为1.29%,平均回收率为100.06%.实际样品的测定证实了该方法的可行性和可靠性.
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| 关 键 词： | 呋喃虫酰肼 高效液相色谱 分析 |
Determination of Pestiside Fufenozide by HPLC |
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| NIE Guo,WU Chun-xian,GA Li-ming,WANG Guang-cheng,CHEN Bin-kun,ZHANG Zhong-ming.Determination of Pestiside Fufenozide by HPLC[J].Journal of Southwest China Normal University(Natural Science),2009,34(6). |
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| Authors: | NIE Guo WU Chun-xian GA Li-ming WANG Guang-cheng CHEN Bin-kun ZHANG Zhong-ming |
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| Abstract: | ;An HPLC method was used to quantitatively analyze the active ingredient of fufenozide by RP-HPLC method.The condition of RP-HPLC method;The mobile phase was methanol +water (70 + 30,by volume).Column temperature was 30℃ ,flow rate was 1.0mL/min,and detection wavelength was 202 nm.The results showed that the linear correlation coefficient was 0.999 9,the standard deviation was 0.14,the variation coefficient was 1.29%,the average recovery was 100.06%.The detection of actual samples proved out that the analytical method was feasible and reliable. |
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| Keywords: | fufenozide HPLC analysis |
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