Reaction of acetylacetone with cyanamide in the presence of catalytic amounts of nickel acetylacetonate |
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| Authors: | V. A. Dorokhov M. F. Gordeev V. S. Bogdanov |
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| Affiliation: | (1) N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, Moscow |
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| Abstract: | Conclusions The reaction of acetylacetone with cyanamide in the presence of Ni(acac)2 involves the addition of the CH2 group at the nitrile group of cyanamide with the formation of 3-(diaminomethylene)pentane-2,4-dione (III) and the products of its transformations, namely, N-acylketenaminals (IV) and (V).Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 6, pp. 1431–1434, June, 1988. |
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