| (烷基环戊二烯基)环戊二烯基二氯化钛的合成与反应 |
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| 引用本文： | 陈寿山,李金山,王积涛.(烷基环戊二烯基)环戊二烯基二氯化钛的合成与反应[J].高等学校化学学报,1986,7(4):322. |
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| 作者姓名： | 陈寿山 李金山 王积涛 |
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| 作者单位： | 南开大学元素有机化学研究所 |
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| 摘 要： | Richard在1959年合成了第一个环戊二烯基(取代环戊二烯基)钛衍生物,(CH3C5H4)(C5H5)T1Cl21].我们曾报道了环戊二烯基(烯烃基环戊二烯基)二卤化钛的合成和反应2]。
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| 收稿时间： | 1984-11-20 |
Synthesis and Reaction of (Alkylcyclopentadienyl) Cyclopentadienyltitanium Dichloride |
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| Chen Shoushan,Li Jinshan,Wang Jitao.Synthesis and Reaction of (Alkylcyclopentadienyl) Cyclopentadienyltitanium Dichloride[J].Chemical Research In Chinese Universities,1986,7(4):322. |
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| Authors: | Chen Shoushan Li Jinshan Wang Jitao |
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| Institution: | Institute of Elemento-Organio Chemistry, Nankai University, Tianjin |
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| Abstract: | The (alkylcyclopentadienyl)cyclopcntadienyltitamum dichloridc, (η5-RC5H4)· C5H5TiCl2 (where R = CH5, C2H5, n-C5H7, n-C4H9, n-C5H11) have been prepared. By exchange reaction of halogen, the corresponding difluoride, dibro-mide and dithiocyanide have been obtained. Their 1H NMRspectrum has also been studied. |
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