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Intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione under the Mitsunobu reaction conditions
Authors:Yu Xia Da  Zhang Zhang  Zheng Jun Quan Key Laboratory of Eco-Environment-Related Polymer Materials  Ministry of Education  Gansu Key Laboratory of Polymer Materials  College of Chemistry  Chemical Engineering  Northwest Normal University  Lanzhou  China
Institution:Key Laboratory of Eco-Environment-Related Polymer Materials, Ministry of Education, Gansu Key Laboratory of Polymer Materials, College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070, China
Abstract:A self-intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione(DHPM) to give a novel tricyclic structure containing DHPM core in the presence of diethyl azodicarboxylate(DEAD) and triphenylphosphine(TPP) at room temperature is reported.
Keywords:Mitsunobu reaction  Cyclocondensation  3  4-Dihydropyrimidine-2-thiones  
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