Synthesis and characterization of bis(cyclopentadienyl)bis(hexafluoroantimonato) titanium(IV) |
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| Affiliation: | 1. CEA, LIST, Software Reliability and Security Laboratory, P.C. 174, Gif-sur-Yvette, 91191, France;2. LAMIH, University of Valenciennes and Hainaut-Cambrésis, 59300 Valenciennes, France;3. Sherpa Engineering, 12 avenue de Verdun, F-92250 La Garenne-Colombes, France;4. ALL4TEC - Immeuble Odyssée - Bât E - 2-12 rue du Chemin des Femmes, 91300 MASSY, France;5. Continental Automotive France SAS, Division I B&S, PG3 CFT, 1 Avenue Paul Ourliac, 31036 Toulouse, France;1. Department of Chemistry, Faculty of Science, Minya University, Minya, Egypt;2. Department of Chemistry, Florida Institute of Technology, Melbourne, FL, USA;1. Laboratory of Physical Chemistry of Materials (LR01ES19), Faculty of Sciences of Monastir, University of Monastir, Avenue de l''environnement, Monastir 5019, Tunisia;2. Faculty of Pharmacy, Laboratory of Medical and Molecular Parasitology-Mycology (LP3M), University of Monastir, LR12ES08, Monastir 5000, Tunisia;3. Département de Chimie Moléculaire, Université Grenoble Alpes, 301 rue de la Chimie, CS 40700, Cedex 9, Grenoble 38058, France;4. Institute of Chemical Sciences of Rennes, UMR 6226, University of Rennes 1, Beaulieu Campus, Rennes 35042, France;5. Faculty of Chemistry, Wroclaw University of Science and Technology, Wybrzeże Wyspiańskiego 27, Wrocław 50-370, Poland |
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| Abstract: | Reaction of titanocene dichloride with two equivalents of silver hexafluoroantimonate in sulphur dioxide quantitatively yields Cp2Ti(SbF6)2 (Cp = η5-C5H5) and AgCl. The titanocene bishexafluoroantimonate was recrystallized from SO2 and characterized by chemical analysis, 1H NMR, IR and mass spectroscopy. |
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