Organosulphur compounds-XXXVIII Axial preference of a 2-dimethoxyphosphoryl substituent in 1,3,5-trithiane |
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| Authors: | Marian Mikokajczyk Piotr Bakczewski Krzysztof Wroblewski Janina Karolak-Wojciechowska Andrzej Miller Michał W Wieczorek Michail Y Antipin Yurij T Struchkov |
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| Institution: | Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences, Department of Organic Sulphur Compounds, 90-362 ?öd?, Boczna 5 Poland;Institute of General Chemistry, Technical University, 90-924 ?öd?, Zwirki 36, Poland;Institute of Organoelement Compounds, Academy of Sciences USSR, Moscov 117312, Vavilov Street 28, USSR |
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| Abstract: | 1H-NMR studies and X-ray analysis indicate that 2-dimethoxyphosphoryl-1,3,5-trithiane exists both in solution and in the crystal in a chair conformation with the dimethoxyphosphoryl group at C-2 being axial. |
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