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A short,efficient total synthesis of (±) acivicin and (±) bromo-acivicin |
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| Authors: | D.M. Vyas Y. Chiang T.W. Doyle |
| Affiliation: | Bristol-Myers Company, Pharmaceutical Research and Development Division Syracuse, New York 13221-4755 U.S.A. |
| Abstract: | A practical approach to the synthesis of (±) acivicin (1) and (±) bromo-acivicin (6) has been developed. It centers on the synthesis of alkene 10 by a thermal [3,3] sigmatropic rearrangement of trichloroimidate 9. |
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