| Mild and Efficient Synthesis of 1-（6-Chloroquinoxalin-2-yl）-2- [4-（trifluoromethyl）-2,6-dinitrophenyl] Hydrazine Derivatives by Microwave Irradiation |
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| 引用本文： | MILAD Taheri,HANIYEH Alavi,HAMIDEH Nazari. Mild and Efficient Synthesis of 1-（6-Chloroquinoxalin-2-yl）-2- [4-（trifluoromethyl）-2,6-dinitrophenyl] Hydrazine Derivatives by Microwave Irradiation[J]. 高等学校化学研究, 2014, 30(3): 405-408. DOI: 10.1007/s40242-014-3417-3 |
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| 作者姓名： | MILAD Taheri HANIYEH Alavi HAMIDEH Nazari |
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| 作者单位： | Department of Chemistry, Islamic Azad University, Tehran 14735/334, Iran |
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| 基金项目： | Acknowledgements The Authors are thankful to Dr. Sozangarzade Head S., Department of Chemistry of Islamic Azad University for availing necessary facilities and valuable guidance. |
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| 摘 要： | Some 1-（6-chloroquinoxalin-2-yl）-2-[4-（trifluoromethyl）-2,6-dinitrophenyl] hydrazine derivatives have been synthesized via both conventional and microwave assisted organic synthesis（MAOS） methods. The MAOS method is more effective on synthesizing these compounds than the conventional method in regard to the higher chemical yields of products（76%-98%） and the shorter reaction time（1-15 min）.
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| 关 键 词： | 高效合成 三氟甲基 肼衍生物 喹喔啉 微波辐射 二硝基苯 氯 有机合成 |
| 收稿时间： | 2013-09-30 |
Mild and Efficient Synthesis of 1-(6-Chloroquinoxalin-2-yl)-2-[4-(trifluoromethyl)-2,6-dinitrophenyl] Hydrazine Derivatives by Microwave Irradiation |
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| MILAD Taheri,HANIYEH Alavi,HAMIDEH Nazari. Mild and Efficient Synthesis of 1-(6-Chloroquinoxalin-2-yl)-2-[4-(trifluoromethyl)-2,6-dinitrophenyl] Hydrazine Derivatives by Microwave Irradiation[J]. Chemical Research in Chinese University, 2014, 30(3): 405-408. DOI: 10.1007/s40242-014-3417-3 |
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| Authors: | MILAD Taheri HANIYEH Alavi HAMIDEH Nazari |
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| Affiliation: | Department of Chemistry, Islamic Azad University, Tehran 14735/334, Iran |
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| Abstract: | Some 1-(6-chloroquinoxalin-2-yl)-2-[4-(trifluoromethyl)-2,6-dinitrophenyl] hydrazine derivatives have been synthesized via both conventional and microwave assisted organic synthesis(MAOS) methods. The MAOS method is more effective on synthesizing these compounds than the conventional method in regard to the higher chemical yields of products(76%―98%) and the shorter reaction time(1―15 min). |
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| Keywords: | 2,6-Dichloroquinoxaline 2-Chloro-1-3-dinitro-5-triflouromthylbenzene hydrazine hydrate Methyl hydrazine Microwave assistant organic synthesis（MAOS） |
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