Synthesis and the structure of the triphenylphosphine complex of o-nickelacarborane, 3,3-(PPh3)2-3,1,2-NiC2B9H11 |
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Authors: | Erdman A. A. Zubreichuk Z. P. Knizhnikov V. A. Maier A. A. Aleksandrov G. G. Nefedov S. E. Eremenko I. L. |
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Affiliation: | (1) Institute of Chemistry of New Materials, National Academy of Sciences of Belarus, 36 Staroborisovskii trakt, 220141 Minsk, Belarus;(2) Institute of Physical Organic Chemistry, National Academy of Sciences of Belarus, 13 ul. Surganova, 220072 Minsk, Belarus;(3) N. S. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 31 Leninsky prosp., 119991 Moscow, Russian Federation |
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Abstract: | The reaction of bis(o-dicarbollyl)nickel(iv) with PPh3 in EtOH gave rise to the complex 3,3-(PPh3)2-3,1,2-NiC2B9H11 (2) whose structure was established by X-ray diffraction analysis. |
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Keywords: | metallocarboranes X-ray diffraction analysis |
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