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Synthesis and the structure of the triphenylphosphine complex of o-nickelacarborane, 3,3-(PPh3)2-3,1,2-NiC2B9H11
Authors:Erdman  A. A.  Zubreichuk  Z. P.  Knizhnikov  V. A.  Maier  A. A.  Aleksandrov  G. G.  Nefedov  S. E.  Eremenko  I. L.
Affiliation:(1) Institute of Chemistry of New Materials, National Academy of Sciences of Belarus, 36 Staroborisovskii trakt, 220141 Minsk, Belarus;(2) Institute of Physical Organic Chemistry, National Academy of Sciences of Belarus, 13 ul. Surganova, 220072 Minsk, Belarus;(3) N. S. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 31 Leninsky prosp., 119991 Moscow, Russian Federation
Abstract:The reaction of bis(o-dicarbollyl)nickel(iv) with PPh3 in EtOH gave rise to the complex 3,3-(PPh3)2-3,1,2-NiC2B9H11 (2) whose structure was established by X-ray diffraction analysis.
Keywords:metallocarboranes  X-ray diffraction analysis
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