Synthesis of 4-(2,2-dibromovinyl)phenol and its one-pot esterification |
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| Authors: | Wensheng Zhang Wenjing Xu Fei Zhang Jitao Li Mei Liu Wei Li |
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| Affiliation: | 1. School of Biological and Chemical Engineering, Jiaozuo Teachers?? College, Shanyang Road 998, Jiaozuo, 450001, China
2. Jiaozuo Vocational Education Center, Huayuan Road 57, Jiaozuo, 454001, China
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| Abstract: | In situ treatment of 4-(2,2-dibromovinyl)phenol, which was prepared from 4-hydroxybenzaldehyde and carbon tetrabromide in CH2Cl2 under Corey?CFuchs conditions, with a diverse range of acids in the presence of dicyclohexylcarbodiimide (DCC) and 4-dimethylaminopyridine (DMAP) gave the corresponding esters in high yields. |
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